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Wysłany: Pon 2:58, 28 Lut 2011 Temat postu: mbt scarpe prezzi Bile pills Weishu process and qu |
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Bile pills Weishu process and quality control of music
On to a methanol chloroform ~ a formic acid ethyl acetate (40:5: select the original drug medicine processing API net I Two I sub-boiling water 2 crushed,[link widoczny dla zalogowanych], over 100} C 『powder + powder three semi-liquid product flow chart of Chinese Folk Medicine No. 86 of 2007 total sieve 10:0.2) as the agent,[link widoczny dla zalogowanych], started out, dried, sprayed with 10% sulfuric acid in ethanol, at 105c 【= heated to a spot color clear. Test products for chromatography, chromatography with reference substance corresponding position, was the same color of the spots. TLC spots corresponding to the good,[link widoczny dla zalogowanych], the draft standard closed set (see Figure 1). TGP 123456 Figure 1 TLC 1. Negative control 2.6. 3.4.5 Paeoniflorin the test temperature: 18 ℃ Relative Humidity: 48% (2) to take this product 10g, methanol 30m1. Ultrasonic treatment 15min, filtered, the filtrate evaporated and the residue add 20ml of water allows the dissolved, with the strong ammonia solution to adjust pH value of 8 to 10. Shake extraction with ether 3 times 15ml, combined ether solution, evaporated and the residue Dissolve 1ml methanol as the test solution. Take tetrahydropalmatine reference substance, add methanol produced per 1ml of solution containing 1mg, as the reference solution. According to thin layer chromatography (6:0.2 m1) as the agent, started out, hanging open, home to the spot of iodine vapor in the smoke color clear. Daylight view. Test products for chromatography, chromatography with reference substance corresponding position, was the same color of the spots; waving in the air to make the board after the adsorption of iodine, UV lamp set (365nm), under review. Test products for chromatography, chromatography with the corresponding position on the reference substance, was the same color of the fluorescent spots. TLC spots corresponding to the good, the draft standard closed set (see Figure 2). 2.3 check: should be consistent with pills under the relevant provisions. (2.4 Indications: blood circulation, gas pain. Indications epigastric pain, pain has given place. Clinical commonly used in acute and chronic gastritis, gastric inflammation, gastric neurosis, and hepatobiliary disease caused epigastric pain. 2.5 Storage: sealed. 2.6 Duration: 1 year and 3 discuss the daylight spectrum fluorescent thin layer map in Figure 2 TLC fumarate 1. Negative control 2. 3.4.5 Tetrahydropalmatine the test room: 20'12 Relative Humidity: 48% of the 3.1 Square Solution of the side by the white peony root, woody herbs such as 6, of which, white peony root: bitter, sour, sweet , slightly cold, in the final by the liver and spleen, nourishing menstruation, Pinggan pain, grabbing Yam Deodorant, modern pharmacological studies, has antispasmodic, analgesic, anticonvulsant, blood pressure, dilation of blood vessels and so on, King and medicine. Woody, Taiwan, Ukraine: acrid, warm, Tonggui stomach through, can manage gas pain, for a total of Robinson medicine, modern pharmacological studies, with the promotion of digestive juice secretion, relaxation of smooth muscle, the gastrointestinal tract with a two-way role of excitatory or inhibitory. Sandalwood, Cyperus rotundus: acrid, warm, Tonggui stomach through, can liver and gas, and cold pain, for a total of adjuvant. Yuan Hu: acrid,[link widoczny dla zalogowanych], bitter, warm, owned by the liver and spleen, to blood circulation, gas, pain,[link widoczny dla zalogowanych], for the adjuvant. Various drugs, played a total of qi and blood circulation, eliminate the plot of stagnation, priorities analgesic power. For the treatment of blood stasis of the stomach pain, rib pain, abdominal pain. 3.2 technology, quality standards that prescribe the composition of the products are mostly spicy, multi-containing volatile compounds, with the raw powder were drugs to live up to their effectiveness, licorice root water decoction, one flavor, the other to reduce the volume. After several clinical trials of its technology is better and stable quality. By thin layer test, the white peony (Paeonia glycosides), Corydalis (Tetrahydropalmatine) to identify better, so I chose this method for making process.
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